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A Guide to High-Quality Microstructural Characterization: Preparation and EBSD Analysis of TC4 (Ti-6Al-4V)

TC4 (Ti-6Al-4V): From Metallographic Preparation to EBSD Characterization

TC4 is a widely used α+β titanium alloy. Reliable microstructural characterization begins with controlled sample preparation.

In the polished condition, metallographic examination can reveal pores, inclusions, cracks, and other defects.

TC4 polished or etched microstructure

After etching, the α and β phases can be differentiated more clearly for microstructural evaluation.

TC4 microstructural evaluation

Preparation Route

  • Grinding: MET-F P400 → P800 → P1200 → P2500
  • Rough Polishing: YS + 3 μm PD-WT
  • Fine Polishing: SC + 1 μm PD-WT
  • Vibratory Polishing: ZN + 50 nm SO-A439

EBSD Characterization & Summary

For EBSD analysis, the final vibratory polishing step is particularly important. It helps reduce the deformation layer remaining from mechanical preparation, improving the surface condition for clear diffraction patterns and reliable indexing.

From metallographic examination to EBSD characterization, good results start with a well-prepared surface.

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